Preparation of Corundum Based Composite Ceramics Using Bauxite Tailings and Vanadium−titanium Magnetite Tailings as Raw Materials

CHEN Jinglong; LANG Zengrui; YANG Fan; CHEN Xinyi; MIN Xin; FANG Minghao; HUANG Zhaohui; HUANG Feihui

doi:10.13779/j.cnki.issn1001-0076.2024.02.014

2024 Vol. 44, No. 2

Article Contents

Article navigation > Conservation and Utilization of Mineral Resources > 2024 > 44(2): 99-105

Next Article Previous Article

CHEN Jinglong, LANG Zengrui, YANG Fan, CHEN Xinyi, MIN Xin, FANG Minghao, HUANG Zhaohui, HUANG Feihui. Preparation of Corundum Based Composite Ceramics Using Bauxite Tailings and Vanadium−titanium Magnetite Tailings as Raw Materials[J]. Conservation and Utilization of Mineral Resources, 2024, 44(2): 99-105. doi: 10.13779/j.cnki.issn1001-0076.2024.02.014

Citation:

CHEN Jinglong, LANG Zengrui, YANG Fan, CHEN Xinyi, MIN Xin, FANG Minghao, HUANG Zhaohui, HUANG Feihui. Preparation of Corundum Based Composite Ceramics Using Bauxite Tailings and Vanadium−titanium Magnetite Tailings as Raw Materials[J]. Conservation and Utilization of Mineral Resources, 2024, 44(2): 99-105. doi: 10.13779/j.cnki.issn1001-0076.2024.02.014

Preparation of Corundum Based Composite Ceramics Using Bauxite Tailings and Vanadium−titanium Magnetite Tailings as Raw Materials

1.
School of Materials Science and Technology, Engineering Research Center of Ministry of Education for Geological Carbon Storage and Low Carbon Utilization of Resources, Beijing Key Laboratory of Materials Utilization of Nonmetallic Minerals and Solid Wastes, National Laboratory of Mineral Materials, China University of Geosciences (Beijing), Beijing 100083, China
2.
Lingyuan Iron and Steel Co., LTD., Lingyuan 122504, Liaoning, China
3.
Shandong Aofu Environmental Technology Co., Ltd., Dezhou 251599, Shandong, China

More Information

Corresponding author: MIN Xin, minx@cugb.edu.cn

Received Date: 09 November 2022

Publish Date: 15 April 2024

Abstract

Abstract

The corundum based composite ceramics were prepared via a high temperature sintering process, using the bauxite tailings and vanadium−titanium magnetite tailings as raw materials. The effects of vanadium−titanium magnetite tailings addition and sintering temperature on the phase composition, morphology, and mechanical properties of the as−prepared composite ceramics were investigated in detail. The results indicated that the best performances were observed with the content ratio of 9∶1 between bauxite tailings and vanadium−titanium magnetite, after sintering at 1 100 ℃ for 3 h. The optimized volume density, compressive strength, and flexural strength were 2.71 g/cm³, 276.9 MPa, and 67.3 MPa, respectively.
- bauxite tailings /
- vanadium−titanium magnetite tailings /
- sintering temperature /
- mechanical property /
- corundum based composite ceramics

FullText(HTML)

References

[1]	李玲, 杨超. 利用尾矿作为建材原料的研究进展[J]. 建材发展导向, 2014, 12(16): 63−67. Google Scholar LI L, YANG C. Research progress on using tailings as building materials[J]. Development Guide to Building Materials, 2014, 12(16): 63−67 Google Scholar
[2]	邢益强, 吴晓鹏, 潘孟博, 等. 铝矾土尾矿基陶瓷透水砖的制备及其性能研究[J]. 中国陶瓷, 2021, 57(2): 46−54. Google Scholar XING Y Q, WU X P, PAN M B, et al. Research on preparation and performance of bauxite tailings−based ceramic permeable brick[J]. China Ceramics, 2021, 57(2): 46−54. Google Scholar
[3]	韩跃新, 柳晓, 何发钰, 等. 我国铝土矿资源及其选矿技术进展[J]. 矿产保护与利用, 2019, 39(4): 151−158. Google Scholar HAN Y X, LIU X, HE F Y, et al. Current situation of bauxite resource and its beneficiation technology in China[J]. Conservation and Utilization of Mineral Resources, 2019, 39(4): 151−158. Google Scholar
[4]	谢武明, 楼匡宇, 张文治, 等. 铝土矿选尾矿制备烧结砖的试验研究[J]. 新型建筑材料, 2013, 40(7): 43−45. doi: 10.3969/j.issn.1001-702X.2013.07.013 CrossRef Google Scholar XIE W M, LOU K Y, ZHANG W Z, et al. Utilization of bauxite tailings in manufacture of fired bricks[J]. New Building Materials, 2013, 40(7): 43−45. doi: 10.3969/j.issn.1001-702X.2013.07.013 CrossRef Google Scholar
[5]	YALLEY PETER PAA−KOFI, ASIEDU EMMANUEL, MPAE ISAAC. Effects of bauxite tailings as partial replacement for sand in sandcrete bricks production[J]. Civil & Environmental Research, 2014, 6(11): 23−30. Google Scholar
[6]	勾密峰, 黄飞, 王思军, 等. 煅烧铝土矿尾矿对水泥凝结时间的影响[J]. 材料导报, 2015(18): 100−102,112. Google Scholar GOU M F, HUANG F, WANG S J, et al. Effect of calcined bauxite tailings on the setting time of cement[J]. Materials Review, 2015(18): 100−102,112. Google Scholar
[7]	申献江, 马冬阳, 张梅, 等. 铝土矿尾矿除杂及合成刚玉−莫来石研究[J]. 耐火材料, 2017, 51(4): 256−259. Google Scholar SHEN X J, MA D Y, ZHANG M, et al. Synthesis of corundum−mullite composites from impurity−removed bauxite tailings[J]. Refractories, 2017, 51(4): 256−259. Google Scholar
[8]	YANG D, FENG N X, WANG Y N, et al. Preparation of primary Al−Si alloy from bauxite tailings by carbothermal reduction process[J]. Transactions of Nonferrous Metals Society of China, 2010, 20(1): 147−152. doi: 10.1016/S1003-6326(09)60112-6 CrossRef Google Scholar
[9]	SHEN X J, QIU G B, YUE C S, et al. Multiple copper adsorption and regeneration by zeolite 4A synthesized from bauxite tailings[J]. Environmental Science and Pollution Research, 2017, 24(27): 21829−21835. doi: 10.1007/s11356-017-9824-5 CrossRef Google Scholar
[10]	LU Q H, HU Y H. Synthesis of aluminum tripolyphosphate anticorrosive pigment from bauxite tailings[J]. Transactions of Nonferrous Metals Society of China, 2012, 22(2): 483−488. doi: 10.1016/S1003-6326(11)61202-8 CrossRef Google Scholar
[11]	童秋桃. 利用铝土矿浮选尾矿制备氧化铝和絮凝剂的研究[D]. 长沙: 中南大学, 2013 Google Scholar TONG Q T. Research on preparation of aluminum oxide and flocculant from bauxite tailing[D]. Changsha: Central South University, 2013. Google Scholar
[12]	刘三军, 刘永, 李向阳, 等. 用铝土矿选矿尾矿制备聚合氯化铝及污水处理试验研究[J]. 湿法冶金, 2020, 39(6): 539−542. Google Scholar LIU S J, LIU Y, LI X Y, et al. Preparation of polyaluminum chloride using bauxite tailings and its application in wastewater treatment[J]. Hydrometallurgy of China, 2020, 39(6): 539−542. Google Scholar
[13]	刘三军, 刘永, 李向阳, 等. 铝土矿尾矿制备聚合氯化铝的浸出试验研究[J]. 衡阳:南华大学学报(自然科学版), 2020, 34(4): 54−57+65. Google Scholar LIU S J, LIU Y, LI X Y, et al. Experimental study on leaching of poly aluminium chloride (PAC) from bauxite tailings[J]. Hengyang: Journal of Nanhua University(Science & Technology), 2020, 34(4): 54−57+65. Google Scholar
[14]	RUAN W Q, GOU M F, LIAO J G. Effect of NaOH solution on performance of aerated concrete containing bauxite tailings[J]. Non−metalic Mines, 2021, 44(6): 38−41. Google Scholar
[15]	MA D Y, WANG Z D, GUO M, et al. Feasible conversion of solid waste bauxite tailings into highly crystalline 4A zeolite with valuable application[J]. Waste Manage ment, 2014, 34(11): 2365−2372. doi: 10.1016/j.wasman.2014.07.012 CrossRef Google Scholar
[16]	ZHANG M, GUO M, WANG Z D, et al. Method for preparing 4A molecular sieve from bauxite tailings: CN102976353A[P]. 2013−03− 20. Google Scholar
[17]	杨帆, 王淇, 闵鑫, 等. 低品位锂辉石对铝矾土尾矿制备莫来石基复相陶瓷的影响[J]. 金属矿山, 2022(9): 244−250. Google Scholar YANG F, WANG Q, MIN X, et al. Influence of low grade spodumene on preparation of mulite−based compound ceramics with bauxite tailings[J]. Metal Mine, 2022(9): 244−250. Google Scholar
[18]	李悦. 利用铝矾土尾矿制备过滤多孔陶瓷[J]. 轻金属, 2016(3): 9−12. Google Scholar LI Y. Production of porous ceramic for filtration by using bauxite tailings[J]. Light Metals, 2016(3): 9−12. Google Scholar
[19]	张翱, 闵鑫, 王淇, 等. 铝土矿尾矿直接烧成制备陶瓷材料及其力学性能研究[J]. 矿产保护与利用, 2022, 42(4): 121−127. Google Scholar ZHANG A, MIN X, WANG Q, et al. Study on the direct firing of bauxite tailings to prepare ceramic materials and their mechanical properties[J]. Conservation and Utilization of Mineral Resources, 2022, 42(4): 121−127. Google Scholar
[20]	REN Y P. Reaction mechanism of porous ceramics prepared from steel slag and bauxite tailings[J]. Metallurgical Engineering, 2018, 5(4): 137−144. doi: 10.12677/MEng.2018.54019 CrossRef Google Scholar
[21]	陈新义, 房明浩, 王淇, 等. 赤泥低温烧结制备长石—刚玉质复相陶瓷[J]. 矿产保护与利用, 2021, 41(6): 103−111. Google Scholar CHEN X Y, FANG M H, WANG Q, et al. Low−temperature preparation of feldspar−corundum composite ceramics from red mud[J]. Conservation and Utilization of Mineral Resources, 2021, 41(6): 103−111. Google Scholar
[22]	李林, 姜涛, 陈超, 等. 攀西钒钛磁铁矿尾矿制备储水泡沫陶瓷的研究[J]. 矿产综合利用, 2020(6): 7−13+6. Google Scholar LI L, JIANG T, CHEN C, et al. Study on preparation of water-retaining foam ceramics from vanadium titanium magnetite tailings[J]. Multipurpose Utilization of Mineral Resources, 2020(6): 7−13+6. Google Scholar
[23]	王维清, 张杰, 朱欣宇, 等. 全尾矿基轻质发泡陶瓷的制备及正交试验研究[J]. 非金属矿, 2022, 45(1): 90−93+97. Google Scholar WANG W Q, ZHANG J, ZHU X Y, et al. Orthogonal experimental study on the preparation of lightweight foamed ceramics by tailings[J]. Non−metallic Mines, 2022, 45(1): 90−93+97. Google Scholar
[24]	陈桃, 简胜, 谢贤, 等. 钒钛磁铁矿尾矿综合利用研究进展[J]. 矿产保护与利用, 2021, 41(2): 174−178. Google Scholar CHEN T, JIAN S, XIE X, et al. Research progress on comprehensive utilization of vanadium−titanium magnetite tailings[J]. Conservation and Utilization of Mineral Resources, 2021, 41(2): 174−178. Google Scholar
[25]	刘长淼, 吴东印, 吕子虎, 等. 某钒钛磁铁矿尾矿中钛铁矿的选矿研究[J]. 中国矿业, 2015, 24(5): 115−117+128. doi: 10.3969/j.issn.1004-4051.2015.05.025 CrossRef Google Scholar LIU C M, WU D Y, LV Z H, et al. Study on recovering ilmenite from V−Ti magnetite tailings[J]. China Mining Magazine, 2015, 24(5): 115−117+128. doi: 10.3969/j.issn.1004-4051.2015.05.025 CrossRef Google Scholar
[26]	宋晓敏, 王永刚. 承德双塔山某尾矿综合回收钛、铁试验[J]. 现代矿业, 2015, 31(1): 86−87+121. Google Scholar SONG X M, WANG Y G. Comprehensive recovery of titanium and iron from a tailings in Shuangtashan, Chengde[J]. Modern Mining, 2015, 31(1): 86−87+121. Google Scholar