Citation: | KONG Jianjun, CHEN Huijie, ZHANG Ming, WEI Kai, CHENG Feifei. Experimental Study on Comprehensive Recovery of Quartz and Feldspar from a Tailings of Tungsten and Tin Gravity Separation in Jiangxi[J]. Conservation and Utilization of Mineral Resources, 2022, 42(6): 146-152. doi: 10.13779/j.cnki.issn1001-0076.2022.07.019 |
According to the characteristics of high content of quartz, feldspar and mica in the tailings of tungsten and tin gravity separation from Jiangxi Province, a fluoride-free and less acid process of grinding-iron removal by magnetic separation-desliming-mica floatation-quartz and feldspar flotation separation was adopted to comprehensively recover quartz and feldspar. Magnetic separation was carried out with the sample grinding fineness of −0.074 mm content 73% and the magnetic field intensity of 1.0 T, following the fine mud of −0.020 mm removed by static-siphon method for non-magnetic products. Furthermore, the mica was floated using a combination of YF-1 (240 g/t) and dodecylamine (80 g/t) as collectors while the slurry pH was adjusted to 10.5 by Na2CO3. Subsequently, quartz and feldspar were separated from mica flotation tailings using Ba2+ as the activator of quartz (120 g/t), YF-2 as the inhibitor of feldspar (250 g/t), and YF-1 as the collector (250 g/t). The flotation tailings was feldspar concentrate, and the flotation concentrate was further separated to obtain the quartz concentrate and feldspar by-products by reverse flotation feldspar process under acidic conditions. The yield of quartz concentrate was 25.30% with a SiO2 content of 99.20%, and the recovery rate of quartz mineral was 50%. Additionally, the yield of feldspar concentrate was 22.69% with K2O+Na2O content of 13.16%, while the yield of feldspar by-products was 7.68% with the content of K2O+Na2O of 9.23%, and the total recovery of feldspar mineral was 79%. The yield of mica concentrate was 14.50%, with K2O, Na2O, and Al2O3 content of 7.65%, 1.65%, and 16.40%, respectively. The recovery rate of mica mineral was 85%.
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Principle process of comprehensive recovery of quartz and feldspar
pH test results of mica flotation
Ratio test results of YF-1 and dodecylamine
Test results of mica flotation collector dosage
Flotation process of mica
Quartz feldspar separation test flow
Test results of pH value of quartz and feldspar separation
Test results of dosage of the inhibitor
Test results of dosage of the activator
Test results of dosage of the quartz flotation collector
Open-circuit flotation flow of quartz feldspar
The flowsheet of closed-circuit test