Professional Committee of Rock and Mineral Testing Technology of the Geological Society of China, National Geological Experiment and Testing CenterHost
2013 Vol. 32, No. 1
Article Contents

Yu YU, Zhen-yun HE, Zhen-cai MAO, Yi WEI, Xiu-ru YUAN, Jiang-bin LIU. Determination of Tin by Spectral Lines with Different Sensitivity of Alternating Current Arc Emission Spectroscopy[J]. Rock and Mineral Analysis, 2013, 32(1): 44-47.
Citation: Yu YU, Zhen-yun HE, Zhen-cai MAO, Yi WEI, Xiu-ru YUAN, Jiang-bin LIU. Determination of Tin by Spectral Lines with Different Sensitivity of Alternating Current Arc Emission Spectroscopy[J]. Rock and Mineral Analysis, 2013, 32(1): 44-47.

Determination of Tin by Spectral Lines with Different Sensitivity of Alternating Current Arc Emission Spectroscopy

  • Based on the advantages of simultaneous determination of multiple elements by using different spectral lines of Alternating Current Arc Emission Spectroscopy, samples with a large range of Sn contents were simultaneously determined by the major spectral line of 317.502 nm and the minor spectral line of 285.062 nm. The working condition for the GBZ-Ⅱ spectral phase plate light meter was optimized by improving the software function. The 317.502 nm spectral line was selected to measure x~xx μg/g Sn in the sample, while the spectral line of 285.062 nm was selected for the determination of 0.0x%~x% Sn. The established method can simultaneously detect two spectral lines with different sensitivities. According to the advantage of high sensitivity by the alternating current arc emission spectroscopy, the high Sn content sample can be analyzed without any dilution, which avoids contamination and artificial errors.
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  • [1] 岩石矿物分析编写组.岩石矿物分析(第四版 第一分册)[M].北京:地质出版社,2011.

    Google Scholar

    [2] 柳本乐.联合接收发射光谱法同时测定化探样品中的W、Mo、Ag、Sn、Pb[J].地质实验室,1993,9(2): 105-107.

    Google Scholar

    [3] 张文华,石静,张雪梅.发射光谱法测定岩石样品中15个痕量元素[J].地质实验室,1995,11(4): 203-207.

    Google Scholar

    [4] 许晓洁,付军刚,贾喜英.发射光谱法测定化探样品中银锡铅硼[J].西部探矿工程,2002,14(5): 74-76.

    Google Scholar

    [5] 叶晨亮.发射光谱法快速测定银锡铜铅锌钼铍[J].岩矿测试, 2004, 23(3): 238-240.

    Google Scholar

    [6] 孙中华,章志仁,毛英,陈之琰.电弧蒸馏光谱法测定化探样品中痕量银锡铅硼镓[J].岩矿测试,2004,23(2): 153-156.

    Google Scholar

    [7] 爱伦斯L H,著.殷宁万,译.分光化学分析[M].北京:地质出版社,1956: 142-143.

    Google Scholar

    [8] 陈礼宽.单矿物光谱分析中增强剂的选择及机理探讨[J].地质实验室,1996,12(4): 193-197.

    Google Scholar

    [9] 沈瑞平.稀有元素及其矿物量的光谱分析[M].南京:江苏科学技术出版社,1983: 124-127.

    Google Scholar

    [10] 李慧芝,翟殿棠,张谨,裴梅山.发射光谱法同时测定10种稀土元素[J].光谱学与光谱分析,2005,22(9): 1500-1502.

    Google Scholar

    [11] 李慧芝,周长利,罗川南.发射光谱法测定矿样中的铌和钽[J].光谱学与光谱分析,2002,22(5): 843-844.

    Google Scholar

    [12] 熊艳.深孔电极载体蒸馏光谱法测定化探样品中八个易挥发元素[J].岩矿测试,2007,26(5): 425-427.

    Google Scholar

    [13] 曹成东,魏轶,刘江斌.发射光谱法同时测定地球化学样品中微量银铍硼锡铋钼[J].岩矿测试,2010,29(4): 458-460.

    Google Scholar

    [14] 湖北省地质实验研究所.GBZ-Ⅱ型光谱像板测光仪使用手册[Z].1992: 8-23.

    Google Scholar

    [15] 叶家瑜,江宝林.区域地球化学勘察样品分析方法(上册)[M].北京:地质出版社,2004: 298-302.

    Google Scholar

    [16] 张雪梅,张勤.发射光谱发测定勘查地球化学样品中银硼锡钼铅[J].岩矿测试,2006,25(4): 323-326.

    Google Scholar

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