Citation: | LYU Xuecheng, SHI Zhonglu, TANG Yongquan, LI Zhiwei. Expansion Experiment of Multi-stage Precision Control Process for Lithium Enrichment in Qarhan Salt Lake Brine[J]. Multipurpose Utilization of Mineral Resources, 2024, 45(4): 50-56. doi: 10.3969/j.issn.1000-6532.2024.04.007 |
This is an article in the field of mining engineering. In view of the concentration and enrichment of lithium ions in old halide in Qerhan Salt Lake, the expansion experiment of the multi-stage precision control process of old halide enrichment was completed by means of evaporation crystallization and step separation. The enrichment law of lithium and boron during evaporation was studied. The concentration of lithium ions reached more than 1 g/L, and high quality hydrochloromagnite was obtained. The material balance of the evaporation process of the salt pan was carried out, and the actual halogen yield and lithium yield of each phase of salt extraction were obtained, as well as the production capacity of the sun salt pan and the area distribution ratio of each level of the salt pan, which can provide reliable data support for the comprehensive development and utilization of potassium old brine extraction in Qerhan Salt Lake in the future.
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Theoretical crystallization roadmap of Qarhan brine evaporation (phase diagram of Li+, Mg2+//Cl-- H2O at 25 ℃)
Multi-stage fine control of salt pan sun drying process
Level 6 test layout of salt pan
Li+ concentration in evaporation process of all levels of salt pans
Boron concentration in evaporation process of all levels of salt pans
Particle size distribution of bischofite in different levels of salt pans