Citation: | Chen Dongli, Luo Qin. Preparation and Characterization of Mullite Microcrystalline Ceramics from Panxi Iron Red Mud[J]. Multipurpose Utilization of Mineral Resources, 2023, 44(5): 204-210. doi: 10.3969/j.issn.1000-6532.2023.05.032 |
This is an essay in the field of ceramics and composites. The microcrystalline ceramics were prepared by a one-step sintering method with kaolin and ferric red mud from Panzhihua, adding potassium feldspar as flux. The microcrystalline ceramics samples were characterized by X-ray diffractometer, Rockwell hardness tester, universal testing machine, electron microscope, thermogravimetric and thermal differential tests. The results show that: When kaolin content is 27%, potassium feldspar content is 25%, red mud content is 55%, sintering temperature is 1250 ℃, holding for 90 min, At this time, the water absorption rate of microcrystalline ceramics is 0.08%, the apparent porosity is 0.15%, the Rockwell hardness is 78.48 HRA, the bending strength is 51 MPa, the main crystal phase is mullite, the grain diameter is less than 6 μm, the grain content can reach 61.35%. The microcrystalline ceramics prepared by this process are dark red, smooth and bright in appearance, and have a warm and moist feeling of jade quality.
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TG-DSC curve of microcrystalline ceramics
Effect of different sintering temperatures on water absorption and apparent porosity
Effect of different sintering temperatures on mechanical properties
Effect of different holding time on mechanical properties
Effect of different holding time on water absorption and apparent porosity
X1000 metallographic of microcrystalline ceramics at different sintering temperatures
XRD patterns of microcrystalline ceramics
Grain size of microcrystalline ceramics
1000X metallographic of microcrystalline ceramics at different sintering temperatures
1000X metallographic of microcrystalline ceramics at different holding times