| Citation: | WANG Qiangqiang, LI Zhenfei, GUO Yuefu, SHEN Xinchun, LAI Jiquan, ZHANG Ting. Experiment on New Comprehensive Recovery of Micro-fine Particle Low-grade Refractory Tantalum Niobium Lithium Resources[J]. Multipurpose Utilization of Mineral Resources, 2025, 46(5): 47-53, 71. doi: 10.12476/kczhly.202409100258 |
The fine-grained low-grade tail mud of the Yichun tantalum niobium ore contains 0.17% Li2O, 0.007 1% Ta2O5, 0.007 8% Nb2O5, and whiteness is 24.20%. Mineralogical studies indicate that tantalum-niobium minerals and lithium mica particles in the tailings are mainly distributed below -20 μm, while feldspar particles are mainly distributed below -45 μm, which is a fine grained and low grade mineral, making resource recovery challenging. Through the beneficiation process of "slurry magnetic separation for iron removal-vibrating cone recovery of tantalum-niobium-flotation to improve feldspar brightness-flotation recovery of lithium mica for the comprehensive recovery of this tailings, experiments achieved a tantalum-niobium concentrate (TaNb)2O5 grade of 27.75%, lithium mica concentrate Li2O grade of 1.57%, with a recovery rate of 42.76%. The feldspar had an Al2O3 grade of 14.92%, Fe2O3 grade of 0.045%, brightness of 68.70%, and total alkali content of 7.91%. This process successfully achieved comprehensive recovery of tantalum-niobium, lithium, and feldspar resources.
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X-ray diffraction (XRD) pattern of the raw ore
Flow of principles
Comparative test results of coarse magnetic field strength
Comparative test results of roughing washing water
Test flow of tantalum niobium recovery
Comparative test flow of different desliming amounts
Comparative test results of different desliming amounts
Test flow of the dosage of collector Zh-2
Test results of the dosage of collector Zh-2
Open-circuit test flow of lepidolite recovery
Closed-circuit test flow of lepidolite recovery
Full process test flow